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HomeMy WebLinkAboutSubmittal HSA AddendumENGINEERS & SCIENTISTS SUBMITTED INTO THE A member of the CRA Family of Companies August 28, 2006 Wilbur Mayorga, P.E. Chief Miami -Dade County Department of Environmental Resources Management Pollution Control Division 33 SW 2"d Avenue, 8th Floor Miami, FL 33130-1540 RE: PUBLIC RECORD FOR ITEMdJ ON , n Site Assessment Report Addendum — Additional Information Knight Ridder — Miami Herald Property (HWR-602/File-22234) Located at, near, or in the vicinity of 1431-1451 North Bayshore Drive Miami, Miami -Dade County, Florida HSA Project No. 801.4385 Dear Mr. Mayorga: HSA Engineers & Scientists (HSA) submitted a Site Assessment Report (SAR) Addendum dated June 27, 2006, to the Miami -Dade County Department of Environmental Resources Management (DERM) for the Miami Herald property at One Herald Plaza, Miami, Florida (site). DERM responded to the SAR Addendum with the August 10, 2006 comment letter included as Attachment A. The following additional information is provided in response to DERM's comments in that letter with the purpose of obtaining No. Further Action without conditions (unconditional NFA) status. All sampling methods performed by HSA were conducted in accordance with the Standard Operating Procedures established by the Florida Department of Environmental Protection. The analytical laboratories used are certified by NELAC. COMMENT 1: DERM acknowledges that utilities to the south of the parking garage impeded further excavation and confirmation sampling; however, based on Figure 7 of the SARA, collection and analysis of a confirmation sample in the grassy area east of the electrical transformer appears feasible. Therefore, advance a soil boring east of the electrical transformer and analyze each two foot interval, to one foot above the water table, for PAHs. www.hsa-env.com Engineering • Environmental Sciences • Construction • Materials Testing 1486-A Skees Road/ West Palm Beach, Florida 33411 Tel: (561) 688-9008 / Fax: (561) 688-9005 Offices in: Tampa • Cape Canaveral • West Palm Beach • Ft. Myers Pensacola • Sunrise • Savannah • Mobile • Biloxi • Hilton Head -m RESPONSE 1: On August 17, 2006, one soil boring (soil boring #1) was advanced in an area east of the electrical transformer. Figure A shows the soil boring location, the electrical transformer and 10-foot set back, underground utilities (electric, communication, and water) and the location of a support column for the overhead mass transit system. Soil samples were collected from the boring in two foot intervals (0-2 feet and 2-4 feet), to one foot above the water table, and submitted for analysis of PAH compounds. The analytical results are summarized on Table 1. PAH compounds were reported below the soil cleanup target levels (SCTLs) for the sample collected in the 0-2 foot interval. The reported benzo(a)pyrene (BAP) concentration (0.41 mg/kg) and the calculated BAP toxicity equivalent concentration (0.54 mg/kg) are below the SCTL for leachability based on groundwater (8 mg/kg) but exceed the default residential direct exposure SCTL (0.1 mg/kg). On August 21, 2006 one soil boring (soil boring #2) was advanced slightly east of the soil boring #1 location and a soil sample was collected from 2-4 feet below land surface (bls, see Figure A). The soil boring could not be advanced at a location further to the east due to the constraint of a concrete footer associated with the support column for the overhead mass transit line (see Figure A). The soil sample was analyzed for PAHs and the reported concentrations of BAP (0.49 mg/kg), dibenz(a, h)anthracene (0.23) and the BAP toxicity equivalent concentration (0.86 mg/kg) are below the SCTL for leachability based on groundwater criteria but exceed the default residential direct exposure SCTL. The analytical data are summarized in Table 1 and the copies of the laboratory reports and sample chain of custody are included in Attachment B. Laboratory results have confirmed that there is no direct exposure risk for the soils in the 0-2 foot interval, and that the soil in 2-4 foot interval contains PAHs at concentrations below the leachability based on groundwater SCTL so impact to the groundwater is not relevant. Therefore, no further action is recommended for the soil south of the parking garage and east of the electrical tiansformer. COMMENT 2: Be advised, the Figure 7 site map identifies analytical results from the 2-4 foot interval for the PGW2560 excavation confirmation samples; however, as per the analytical results submitted with the SARA, this interval was not analyzed. Correct this discrepancy in the next submittal. RESPONSE 2: A revised copy of Figure 7 is attached to correct this discrepancy. SUBMITTED INTO THE PUBLIC RECORD FOR 2 ITEM`°SON . COMMENT 3: The next submittal shall include chain of custody forms for all analytical data submitted with the SARA. RESPONSE 3: Copies of the chain of custody forms for all analytical data submitted with the SARA are provided in Attachment C. This additional information to the Site Assessment Report further documents the soil quality at the Site. Based on the site status and the work completed, we respectfully request a No Further Action without conditions determination be granted for the site. We would appreciate your timely response to the information presented. Please contact us if you have any questions or required additional information. Sincerely, HSA Engineers & Scientists Terrence R. Horan P.E. Number 54815 SUBMITTED INTO THE PUBLIC RECORD FOR ITEMT.;ON1i- ov-oe,. 09/18/2006 14:44 15616889005 HSA ENG & SCIENTISTS PAGE 01 .....•••••••••-• HsA ENGINEERS & SCIENTISTS A Member of the CRA Family of Companies Fax Cover Sheet DATE: 9118/06 NO. OF PAGES (ins cover): 2 TO: Kerri Barsh Company: Greenberg Traurig Phone No.: 305-579-0772 Fax No.: 305-961-5772 FROM: Katrina Greco HSA Engineers & Scientists Phone: (561) 688-9008 Fax: (561) 688-9005 Project / 8014385 Proposal No.: Project 1 Knight Ridder — Miami Herald Property Proposal Name: (HWR-603IFile-2234) Miami, Miami Dade County, Florida If the following message is received poorly or incomplete, please notify us at (561) 688-9008. Comments: Good Afternoon, Please find attached Cover Letter to be included with "Site Assessment Report Addendum — Additional Information', dated August 28, 2006, received by Federal Express. If you have any questions or comments concerning this report, please contact Terry Horan or myself. Thank You, HSA Engineers & Scientists Katrina Greco SUBMITTED INTO THE PUBLIC RECORD FOR ITEV. ON It- . 1486-A Skees Road, West Palm Beach, FL 33411 Tel: (561) 688-9008 Fax: (561) 688-9005 Sample ID: TABLE 1 LABORATORY RESULTS OF SOIL SAMPLES FOR PAH ASSESSMENT EAST OF TRANSFORMER KNIGHT RIDDER - MIAMI HERALD PROPERTY c m ar a L 2-Methylnaphthalene m m 3 0 • • m 1m c .c` m • ea `�° m L c c 0. rc 0 N t7 O• � N C o C t N • 0. N N N , . Q co U Dibenz[a,h]anthracene Fluoranthene Phenanthrene to c Benzo (A) Pyrene Toxic Equiv. 0-2' (Soil Boring #1) 2-4' (Soil Boring #1) <0.3 <0.3 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <0.1 <0.1 <0.1 0.28 <0.1 <0.1 <0.3 <0.3 0.22 <0.3 <0.3 <0.3 <0.1 <0.1 0.37 0.41 0.51 0.36 0.39 0.48 <0.1 0.88 <0.1 0.38 <0.1 0.27 0.64 SB-82106 (Soil Boring #2) (2-4') <0.3 <0.3 <0.3 <0.1 <0.1 0.38 0.49 0.53 0.43 0.48 0.57 0.23 0.88 <0.1 0.47 <0.1 0.18 0,61 <0.1 0.54 0.86 Toxic Equiv. Factor: n/a n/a n/a n/a n/a 0.1 1 0.1 n/a 0.01 0.001 1 n/a n/a 0.1 n/a n/a n/a 1.0 Resid. CTL: 200 210 2,400 1,800 21,000 1.3 0.1 1.3 2,500 13 130 0.1 3,200 2,600 1.3 55 2,200 2,400 0.1 Indus, CTL: 1800 2,100 20,,000 20,000 300,000 6.6 0,7 6.5 52,000 ........6.6 640 0.7 59,000 33,000 6,6 300 36,000 45,000 0.7 FDEPleach.: _ »»__ _.....................�...._.._ ___..._.._.._.................,.......__............__.._........._.._» _..._. Based on Groundwater 3.1 8.5 2.1 27 2 500 0.8 8 2.4 32,000 24 w 7 77 0.7 1,200 160 6.6 1.2 250 880 8 Based on Freshwater Surface Water 10.0 9.1 0.3 NA 0 0.4 NA NA NA NA NA NA NA 1.3 17 NA 2.2 NA 1.3 NA Based on Madn. Surface Water 10.0 9.1 0.3 NA 0.4 NA NA NA NA NA NA NA 1.3 17 NA 2.2 NA 1.3 NA Based on Groundwater of Low yleldrPoor Quality 3 31.0 85.0 21.0 2 270 25,000 8.0 80 24.0 320,000 240 770 70.0 12,000 1,600 66.0 12.0 2,500 8,800 80 Resid. (DERM): . » 93 110.. 22 400 .,. 1,800 21,y000 1.3 0.1 1.3 2 500 .. _13 1 130 0.1 3,200 2,600 1.3 55 2,200 2,400 0.1 Indus. (DERM): .510 610 20 OW20,000 300 000 6.6 0.7 6.5 52 000 _._66_ 6 640 0.7 59,000 33,000 6.6 300 36,000 45,000 0.7 DERM leach. Based on Groundwater 2.2 6.1 2.1 27 2,500 0.8 8 2.4 32,000 25 77 0.7 1,200 160 6.6 1.7 250 880 8 Based on Freshwater Surface Water 10 9.1 0.7 0.7 0.7 0.7 1.2 1.6 4.8 1.6 0,7 4.7 1.3 17 4.3 2.2 0.7 1,3 1.2 Based on Madne Surface Water 10.0 9.1 0.7 0.7 0.7 0.7 1.2 1.6 4.8 1.6 0.7 4.7 1.3 17 4.3 2.2 0.7 1.3 1.2 CTL: Cleanup Target Level All concentrations expressed in mg/kg Bolded values have concentrations greater than the lesser CTL Page 1 of 1 cm W rn re O CC z ® z XI 0 O -� Tj O 0 a7 rr,t • ENGINEERS do SCIENTISTS IMs-* a.•• w u.w ►e.. Mr... .4 11411 ATTACHMENT A DERM Letter from August 10, 2006 SUBMITTED INTO THE PUBLIC RECORD FOR ITEMt'_ON '-b1-ot AOA Coordination Agenda Coordination Animal Services 1s Art in Public Places Audit and Management Services Aviation Building Building Code Compliance Business Development Capital Improvements Citizens' Independent Transportation Trust Commission on Ethics and Public Trust Communications Community Action Agency Community & Economic Development Community Relations Consumer Services • Corrections.& Rehabilitation Cultural Affairs Elections .EmergemyManage Management Employee Relations Empowerment Tnisl Enterprise Technology Services Environmental Resources Management fair Employment Practices finance Fee Rescue General Services Administration Historic Preservation Homeless Tirol Housing Agency Housing finance Authority Human Services Independent Review Panel International Trade Consortium Juvenile Assessment Center Medical Examiner Metro -Miami Action Plan .Metropolitan -Planning Organization Park and Recreation Planning and Zoning Police Procurement Management Property Appraisal Public Library System Public Works Safe Neighborhood Parks Seaport Solid Waste Management Strategic Business Management Team Metro Transit Task Force on Urban Economic Revitalization Vizcaya Museum And Gardens Water & Sewer Environmental Resources Management Pollution Control Division 33 SW 2nd Avenue • 7th Floor Miami, Florida 33130-1540 T 305-372-6700 F 305-372-6729 August 10, 2006 CERTIFIED MAIL NO. 7001 0320 0003 8095 7757 RETURN RECEIPT REQUESTED Larry Marbert VP Production and Facilities Knight Ridder One Herald Plaza, 6th Floor Miami, Florida 33132 miamidade.gov SUBMITTED INTO THE ?UBLIC RECORD FOR TEM?". ON CERTIFIED MAIL NO. 7001 0320 0003 8095 7740 RETURN RECEIPT REQUESTED. P.A. Ridder Miami Herald Publishing Company 50 W San Fernando Street San Jose, California, 95113 RE: Site Assessment Report Addendum (SARA) dated June 27, 2006 and submitted by HSA Engineers & Scientists for the Knight Ridder-Miami Herald Property facility (HWR-602/File-22234) located at, near, or in the vicinity of 1431-1451 North Bayshore Drive, Miami, Miami -Dade County, Florida. Dear Messrs. Marbert and Ridder: The Pollution Remediation Section of the Department of Environmental Resources Management (DERM) has reviewed the referenced submittal, received June 27, 2006 The following is required: 1 DERM acknowledges that utilities to the south off the parking garage impeded further excavation and confirmation sampling; however, based on Figure 7 of the SARA, collection and analysis of a confirmation sample in the grassy area east of the electrical transformer appears feasible. Therefore, advance a soil boring east of the electrical transformer and analyze each two foot interval, to one foot above the water table, for PAHs. 2. Be advised, the Figure 7 site map identifies analytical results from the 2-4 foot interval for the PGW2560 excavation confirmation samples; however, as perthe analytical results submitted with the SARA, this interval was not analyzed. Correct this discrepancy in the next submittal. 3. The next submittal shall include chain of custody forms for all analytical data submitted with the SARA. ATTACHMENT B Soil Sample Analytical Data and Chain of Custody SUBMITTED INTO THE PUBLIC RECORD FOR ITEMIZAi ON . Jupiter crn•imnm?nlal Labor. r ,ri�c. 1ni - August 18, 2006 Terrance Horan HSAEngineers & Scientists 1486-A Skees Rd West Palm Beach, FL 33411 RE: LOG# 616645 Project ID: 8015.4385-03 Knight Ridder COC# 28960 Dear Terrance Horan: Jupiter Envicnmental Laboratories, Inc. ' 50 S. OIA Dixie Highway Jupiter, FL 33458 Phone: (561)575-0030 Fax: (561)575-4118 www.jupderlabs.com cliertservices@jupitedabs.com SUBMITTED INTO THE PUBLIC RECORD FOR ITEMCi ON a-oa-ov. Enclosed are the analytical results for sample(s) received by the laboratory on Thursday, August 17, 2006. Results reported herein conform to the most current NELAC standards, where applicable, unless indicated by • in the body of the report. The endosed Chain of Custody is a component of this package and should be retained with the package and incorporated therein. Results for all solid matrices are reported in dry weight unless otherwise noted. Results for all liquid matrices are reported as received in the laboratory unless otherwise noted. Samples are disposed of after 30 days of their receipt by the laboratory unless archiving is requested in writing. The laboratory maintains the right to charge storage fees for archived samples. Certain analyses are subcontracted to outside NELAC certified laboratories, please see the Footnotes section of this report for NELAC certification numbers of laboratories used. AStatement of Qualifiers is available upon request. If you have any questions concerning this report, please feel free to contact me. Sincerely, Ann Md(ewin for Karla Baldwin kbaldwin@jupiterlabs.com Endosures Report ID: 616645 - 211139 Page 1 of 5 8/18/2006 FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In full, without the written consent of Jupiter Environmental Laboratories, Inc.. c !Pe C'_ Jupiter Environmental Laboratories inc. SAMPLE ANALYTE COUNT LOG# 616645 Project ID: 8015.4385-03 Knight Ridder Jupiter Environmertal Laboratories, Inc. 150 S. Old Dixie Highway Jupiter, FL 33458 Phone: (561)575-0030 Fax: (561)575-4118 Lab 1D Sample ID 616645001 2' 616645002 4' Report ID: 616645 - 211139 8/18/2006 Method EPA 8270C EPA8270C Analyses Reported 21 21 SUBMITTED INTO THE PUBLIC RECORD FOR ITEM ONtI-oq-b. FDOM# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, without the written consent of Jupiter Environmental laboratories, Inc.. `o.r •cr.brr liefA Page 2of5 Jupiter EnviN i:1i?ntal Laboratories, Inc. -SAMPLE SUMMARY LOG# 616645 Project ID: 8015.4385-03 Knight Ridder Jupiter Environmental Laboratories. Inc. 150 S. ad Dixie Highway Jupiter, Ft_ 33458 Phone: (561)575-0030 Fax: (561)575-4118 Lab ID Sample ID Matrix 616645001 2' 616645002 4' Report ID: 616645 - 211139 8/18/2006 Date Collected Date Received SoiUSolid/Sediment 8/17/2006 14:15 8/17/2006 16:20 Soil/Solid/Sediment 8/17/2006 14:45 8/17/2006 16:20 SUBMITTED INTO THE PUBLIC RECORD FOR ITEM,1' ON mo9-040. FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In full, without the written consent of Jupiter Environmental Laboratories, Inc.. halt - Page 3of5 Jupiter Environment:II I_ahor r-,r,P5, InC. ANALYTICAL RESULTS LOG# 616645 Project ID: 8015.4385-03 Knight Ridder Jupiter Environmental Laboratories. Inc. 150 S. ad Dixie Highway Jupiter. FL 33458 Phone: (561)575-0030 Fax: (561)575-4118 Lab ID: 616645001 Sample ID: 2' Date Received: 8/17/2006 Matrix: Soil/Solid/Sediment Date Collected: 8/17/2006 Parameters Results Units Report Limit MDL DF Prepared By Analyzed By Qual CAS SenilvolatIles by EPA 8270C :Analysis Desc.EPA8100 PAii Scan (S) 1-Methylnaphthalene 2-Methylnaphthalene Acenaphthene Ac enephthylene Anthracene Benz(a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo(g,h,i]perylene Benzo(k]fluoranthene Chrysene Dibenz(a,h]anthracene Fluorttrlthene Fluorene Indeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) p-Terphenyl-d14 (S) Report ID: 616645 - 211139 8/18/2006 U U U U U U U u U U U U 0282 U U U U 0.224 99 102 122 Preparation Analytical M mg/Kg' ... mg/Kg mglkg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mglkg mg/Kg mg/Kg mg/Kg mglkg Mg/Kg mg/Kg mg/Kg mglkg Method EPA 3545 ethvd:..EPA 8270C 0.100 0.020 0.100 0.024 0.100 0.100 0.100 0.100 0.100 0.100 0.200 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 20-120 25-120 15-140 0.017 0.019 0.026 0.032 0.033 0.030 0.036 0.037 0.018 0.042 0.021 0.026 0.034 0.020 0.020 0.022 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06. NL 1 08/17/06 TG 08/18/06. NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06. NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 90-12-0 91-57-6 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206-44-0 86-73-7 193-39-5 91-20-3 85-01-8 129-00-0 4165-60-0 321-60-8 1718-51-0 SUBMITTED INTO THE PUBLIC RECORD FOR ITEM?'J ON 1\-09-010. FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In full, without the written consent of Jupiter Environmental laboratories, Inc-. 1 �iQC�: Page 4 of 5 Jupiter invii of i 1eiiijl Laboratories. Iris. ANALYTICAL RESULTS LOG# 616645 Project ID: 8015.4385-03 Knight Ridder Jupiter Environmental Laboratories, Inc. 150 S. Old Dixie Highway Jupiter, FL 33458 Phone: (561)575-0030 Fax: (561)5754118 Lab ID: 616645002 Sample ID: 4' Date Received: 8/17/2006 Matrix: SoillSolid/Sediment Date Collected: 8/17/2006 Parameters Results Units Report Limit MDL DF Prepared By Analyzed By Qual CAS Semivolatiles by EPA 8270C Analysis Desc: EPA8100 PAH Scan (S) 1-Methylnaphthalene 2-Methylnaphthal one Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene eenzo(a)pyrene Benzo[bpluoranthene Benzo(g,h,ijperylene Benzo[k]fluoranthene Chrysene Dibenz[a,hjanthracene Fluoranthene Fluorene Indeno(1,2 ,3-cd]pyrene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-FRuorobiphenyl (S) p-Terphenyld14 (S) Report ID: 616645 - 211139 8/18/2006 Preparation Analytical M U mg/Kg U mg/Kg U mg/Kg U mg/Kg U mg/Kg 0.370 mg/Kg 0.412 mg/Kg 0.505 mg/Kg 0.363 mg/Kg 0.385 mg/Kg 0.480 mg/Kg U mg/Kg 0.877 mg/Kg U mg/Kg 0.384 mg/Kg U mg/Kg 0.274 mg/Kg 0.637 mg/Kg 94 % 92 % 113 % Method: EPA3545: elhod: EPA 8270C 0.100 0.020 0.024 0.017 0.019 0.026 0.032 0.033 0.030 0.036 0.037 0.018 0.042 0.021 0.026 0.034 0.020 0.020 0.022 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.200 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 20-120 25-120 15-140 108/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 1 08/17/06 TG 08/18/06 NL 108/17/06 TG 08/18/06 NL 90-12-0 91-57-6 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206-44-0 86-73-7 193-39-5 91-20-3 85-01-8 129-00-0 4165-60-0 321-60-8 1718-51-0 ;UBMITTED INTO THE 'UBLIC RECORD FOR S ,FM PL. �t i ON k\-oq-w. FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In hill, without the written consent of Jupiter Envronmental Laboratories, lnc.. Page 5of5 Chain of Custody Record Jupiter Environmental Laboratories Company Name c SetE sr5 Address 14 0 —i S City s ' • Livt Be 4. State FL Zip 331/O$ Project Name 6MT'Et ' Project tf : r is; : Zl (r Matrix Codes' S SoiVSolid Sediment SW Surface Water OW around Water SL Sludge WW Waste Water 0 other (Please Specify) DW Drinking Water S�f L tc A• none 1• Ice B- HNC, 0- Other C• H,SO, M• M9OH D- NaOH E- HCI QAJQC level with report None 1 2_ _3See • rice • uide for"ap • livable fees T.A.T. Request Standard sF FDEP___ SFWMD_ Date Required Temp Control: J.E.L. Log # ;� i(✓G'S P.O.# Quote# Comments Time 2 ries, Inc. 150 Old Dixie Highway, Jupiter, FL 33458 (561) 575-0030 • Fax (561) 575-4118 • cilentservicesOjupiteriabs.com Jupiter Environmental Lab c.o.c.# 28960 ORIGINAL PPM. I of Environmental Laboratories, Irx. August 22, 2006 Terrance Horan HSAEngineers & Scientists 1486-A Skees Rd West Palm Beach, FL 33411 RE: LOG# 616655 Project ID: 8014385-03 Knight Ridder COC# 28974 Dear Terrance Horan: Jupiter Environmental Laboratories, Inc 150 S. Old Dixie Highway Jupiter. FL 33458 Phone: (561)575-0030 Fax: (561)575-4118 www.jupiterlabs.com clientservices@jupiteriabs.com SUBMITTED INTO THE PUBLIC RECORD FOR ITEM1'1;07-11 ON it --01-o6. Endosed are the analytical results for sample(s) received by the laboratory on Monday, August 21, 2006. Results reported herein conform to the most current NELAC standards, where applicable, unless indicated by • in the body of the report. The endosed Chain of Custody is a component of this package and should be retained with the package and incorporated therein. Results for aU solid matrices are reported in dry weight unless otherwise noted. Results for all liquid matrices are reported as received in the laboratory unless otherwise noted. Samples are disposed of after 30 days of their receipt by the laboratory unless archiving is requested in writing. The laboratory maintains the right to charge storage fees for archived samples. Certain analyses are subcontracted to outside NELAC certified laboratories, please see the Footnotes section of this report for NELAC certification numbers of laboratories used. •A Statement of Qualifiers is available upon request. tf you have any questions conceming this report, please feel free to contact me. Sincerely, clat&ax Mn McKewin for Kaca Baldwin lcbaldwin@jupiterlabs.com Endosures Report ID: 616655 - 211930 8/22/2006 FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In full, without the wdRen consent of Jupiter EnvonmentaI Laboratories, Inc.. Page1 of 4 Jupiter Jupiter Environmental Laboratories, Inc. 150 S. Oid Dixie Highway Jupiter, FL 33458 Environmental Laboratories, Inc. Phone: (561)575-0030 Fax: (561)5754118 SAMPLE ANALYTE COUNT LOG# 616655 Project ID: 8014385-03 Knight Ridder Lab ID Sample ID Method Analytes Reported 616655001 SB-82106 EPA8270C 21 SUBMITTED INTO THE PUBLIC RECORD FOR ITEMTA v;e ON n-oy -oi,. Report ID: 616655 - 211930 Page 2 of 4 8/22/2006 FDOH# E86546 CERTIFICATE OF ANALYSIS Thls report shall not be reproduced, except In full, without the written consent of Jupiter Environmental Laboratories, Inc.. ;etaC Jupiter Environmental Lalxxarories, Inc. SAMPLE SUMMARY LOG# 616655 Project ID: 8014385-03 Knight Ridder Jupiter Environmental Laboratories, Inc. 150 S. Old Dixie Highway Jupiter, FL 33458 Rhone: (561)575-0030 Fax (561)575-4118 Lab ID Sample ID Matrix 616655001 SB-82106 Report ID: 616655 - 211930 8/22/2006 Soil/Solid/Sediment Date Collected Date Received 8/21/2006 12:15 8/21/2006 14:30 SUBMITTED INTO THE PUBLIC RECORD FOR ITEM utq ON n c51-oc, FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except in full, without the written consent offJJupiter rEEnviroomental Laboratories, Inc.. Page3of4 1-Methylnaphthalene 2-Methylnaphthalene Acenaphthene Acenaphthylene Anthracene Benz(a)anthracene Benzo(a pyrene Benzo(bjtluoranthene B enza(g,h, i)perytene Benzo(k)fluoranthene Chrysene Dibenz(a,hjanthracene Fluoranthene Fluorene hrdeno(1,2,3-cd)pyrene Naphthalene Phenanthrene Pyrene Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) p-Terphenyl-d14 (S) Report ID: 616655 - 211930 8/22/2006 2-- Jupiter • Environmental LahoratorieS, Inc_ ANALYTICAL RESULTS LOG# 616655 Project ID: 8014385-03 Knight Ridder Jupiter Environmental Laboratories, Inc. 150 S. Old Dixie Highway Jupiter, FL 33458 Phone: (561)575-0030 Fax: (561)575-4118 Lab ID: 616655001 Sample ID: SB-82106 Date Received: 8/21/2006 Matrix: SoillSolid/Sediment Date Collected: 8/21/2006 Parameters Results Units Report Limit MDL DF Prepared By Analyzed By Qual CAS Sennivolatiles by EPA 8270C Analysis Dose; 'SPA 8100 PAH Scan (S) =, Preparation Method: EPA3545 Analytical Method: EPA 8270C U mg/Kg 0.100 0.020 1 08/21/06 TG 08/21/06 NL U mg/Kg 0.100 0.024 1 08/21/06 TG 08/21/06 NL U mg/Kg 0.100 0.017 1 08/21/06 TG 08/21/06 NL U mg/Kg 0.100 0.019 1 08/21/06 TG 08/21/06 NL U mg/Kg 0.100 0.026 1 08/21/06 TG 08/21/06 NL 0.379 mg/Kg 0.100 0.032 1 08/21/06 TG 08/21/06 NL 0.486 mg/Kg 0.100 0.033 1 08/21/06 TG 08/21/06 NL 0.532 mg/Kg 0.100 0.030 1 08/21/ 6 TG 08/21/06 NL 0.432 mg/Kg 0.200 0.036 1 08/21/06 TG 08/21/06 NL 0.482 mg/Kg 0.100 0.037 1 08/21/06 TG 08/21/06 NL 0.574 mg/Kg 0.100 0.018 1 08/21/06 TG 08/21/06 NL 0.231 mg/Kg 0.100 0.042 1 08/21/06 TG 08/21/06 NL 0.884 mg/Kg 0.100 0.021 1 08/21/06 TG 08/21/06 NL U mg/Kg 0.100 0.026 1 08/21/06 TG 08/21/06 NL 0.473 mg/Kg 0.100 0.034 1 08/21 /06 TG 08/21 /06 NL U mg/Kg 0.100 0.020 1 08/21/06 TG 08/21/06 NL 0.179 mg/Kg 0.100 0.020 1 08/21/06 TG 08/21/06 NL 0.609 mg/Kg 0.100 0.022 1 08/21/06 TG 08/21/06 NL 65 % 20-120 1 08/21/06 TG 08/21/06 NL 78 % 25-120 1 08/21 /06 TG 08/21 /06 NL 90 % 15-140 1 08/21/06 TG 08/21/06 NL 90-12-0 91-57-6 83-32-9 208-96-8 120-12-7 56-55-3 50-32-8 205-99-2 191-24-2 207-08-9 218-01-9 53-70-3 206.44-0 86-73-7 193-39-5 91-20-3 85-01-8 129-00-0 4165-60-0 321-60-8 1718-51-0 UBMITTED INTO THE 'UBLIC RECORD FOR EMP(.2:17-1 ON I1-o9-010 FDOH# E86546 CERTIFICATE OF ANALYSIS This report shall not be reproduced, except In full, without the written consent of Jupiter Environmental Laboratories, Inc.. Page 4 of 4 Chain of Custody Record Jupiter Environmental Laboratories ( r Company Name F , `Sc J . J.E.L. Log # /Pik) 4'5-5 P.O. # Quote# Project Name `A p Pivrae Project N TZ lay Comments Matrix Codes* S SoiVSolid Sediment SW Surface Water OW Ground Water SL Sludge WW Waste Water 0 other (Please Specify) DW Drinking Water A• nave 1- Ice B- HNC, 0- Other C- H,SO, M- McOH D- NaOH • E• HCI QA! • C level with report None _._•-1 23_-_ See price ! uide for ap • Iicable fees T.A.T. Request FDEP_ Standard SFWMD_ /4. /Rush Date Required Temp Control: °C MN =FROM ME =EKON II MINIMMAMMM MMEMMENUM MnAaEs m mum ImmallEMOMM MEMMEN �4130 Date 1111=1111111111111111 Time 30 ries, Inc. 150 Old Dixie Highway, Jupiter, FL 33458 (561) 575-0030 • Fax (561) 575-4118 • cllentservices@Jupiterlabs.com Jupiter Environmental Lab c.o.c.# 28974 ORIGINAL PADA of I SUBMITTED INTO THE PUBLIC RECORD FOR ITEM ;tp i;" ON ATTACHMENT C SARA Chain of Custody Forms t3ARL'OGE °xr,; Chain of Custody Record Jupiter Environmental Laboratories J.E.L. Log # P.O.# Quote# Company Name ,- •s.,t.... 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Chain of Custody Record 111111111111111111111111111111111111 1111111111111111111111111111111ff 111111111111111111111111111111Wz 01111111111111111111111111111111r7t111111111111111111111111111111111 v4. 111111111111111111111111111111111111111111 odes, Inc. 150 Old Dixie Highway, Jupiter. FL 33458 J.E.L. Log # P.O.# Quote# A 1 A Chain of Custody Record BAR CODE. Jupiter Environmental Laboratories J.E.L. Log # i c ;-(?C P.O. # Quote# Company Name >4.1 w' Address ) 486 A S cY A A- D /r A City W`ki:State Zip 314 11 4 , Q d ` 0 t 5 O '� . ' Sampling Site Address ;; Attn Te / I ^. Fax/Email.s6 t 6,28 se• yet # _ Project �y. � e- _ Name Q� ,C I i Project # L50 L.J � 1.- O }� 444, $ Comments Sampler Name/Signature G„c• t S L. Ae. r •? # .. 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AA.. .. - Chain of Custody Record Jupiter Environmental Laboratories LAB USE ONLY 130 J.E.L. Log # P.O.# Quote# y� Company Name 11 &rok $d6 1 pJ� ' .. <.. .. .t t�°x A 8 dx ,. ....,. , Address / 486A S 4e C_Sb City State CL zip 33Lt1I Sampling Site Address ;' - (�� Attn: )�L+.,/ 'CJIZTr1 Fax/Email Sy.„ � �jg _ rara� t a ��� Q1 � o, c�. Project � (� 1 ` _ �. y Name F^• 4L .e Project N ©i `u 1g —il rt � � . ( � . 0 Sampler C....4.2,,. Name/Sinature �f`S L,-Al f / -a^- :; w' ,s ta # .foli Siam e9 ���. �_� �_ w �� .. k { 3 IIltrix *,. Code` 'to Comments °►: f = PG'''t I -sio. a- i' 3 !6-cad, S7 S [ CI) J ___, 2 worse -s$ao-' lam I -'" rncoC7C ..g. 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(Please DW Drinking Water D• NaOH E• HCI �) , N 919-0 " i2 QA/QC level with report -- / None 12_3_ See price guide for applicable fees ./--_. T.A.T. Request FDEP Standard SFWMD. Rush Date Required Temp Control:17;3_4--' :7._ _. I L f' }el Jupiter Environmental Laboratories, Ine — 1 CA e11.1 fll,.L LIiwku.at. I..wNs. GI P. A A A r. (SQ11 S7s_nnln . Cn.. ICCI' a ,e A4 4 n • ..._.. • ... • . .. nr. Chain of Custody Record BARCS . Jupiter Environmental Laboratories J.E.L. Log # b/54H A P.O. # Quote# 7`�i • Company Name � fir"-: r t ,i, . s ": -.._... : 1'i� r� . ''.�° `�•,e•' ' s Address �� e6 "� 4 ��� Z»P � � t City Li•J• / . 3. State Zip , / / • Sampling Site Address �" %( Attn: PA ' Oidloe6rfli P Fax/Email 0 Project / Name 1W 6 P,P It ojct N �C/55�e7.0, O 5 1 an e� Comments Sampler Name/SignatureW4it, $ Pent') Si 00.4s 2 '''{ SS '2-05- $: l7 Matrix soy 1-- 3 � ` (Jr)11 C -- :. r '-v ,_2 s i 17'2-e°t-SW 8'; Zo '' rn 03 1:43 3 PGe/-.0-z-2�N1 V zz f a.,"1� '1 tbx.i) 1_4 .ZPG0t- z-"-Zc AI g- ( $1;1�XI 145 4v 15 T.'4M/-o-z--zo3 2-=ZP l✓ (gym t t-.1› 16 CP6102-0-Z-t oS 8' .30 1 v Z O Z /-+,(...:T> 7 2'FG&!-2''f Zo 3 Fr: YO rl t,/ L. ---�= � 18 =pc.M/- -zr>nr c .413 i ✓ T -.I 1 9 ,=6M 1-0- 2-- zo a 0-: Y.Sr t L.-'- b Q= HC%Lb 2.0 7?z-o--v/0s 8:5-7, / I t/ wrn Matrix Codes' i '�:� • '�� °' .. �� edify'"< Date Time S SdUSolid Sediment SW Surface Water GW Ground Water SI_ Sludge WW Waste Water 0 Other Specify) A. none I• Ice B- HNC, 0- Other C- H2SO4 M• Me0H 3 "2•Q+ 2 • S (Please DW Drinking Water E- NaOH 1:112._ 03 -1 ? -) C L a QA/QC level with report None 1 23 See price guide for applicable fees ,^ - -t° •O 1'—Cte / 1711 T.A.T. Request FDEP Standard SFWMD_ Temp Control: ,,� .- "'"-- / j, /G/.� /2/1 _ Rush Date Required j C e /t Jupiter Environmental Laboratories, Inc. i =t1 A1.1 1114ria uiwti..... 1..w1•a. CI .1 . i. .. ___ •.._ . rnr++ Chain of Custody Record BAR Jupiter Environmental Laboratories J.E.L. Log # P.O.# Quote# Company Name # .4� a g °' C Address Ns ‘ A st &ob. City w. P 73, State Fe4Zip 33 r // s "Z.. ` Q. -- Sampling Site Address,, / (0 /j�� Att •�dili %�% Fax/Emall Pro)ectj(f i�l r/� P j O � Name roectk c ► Comments Samples Name/Signature��� ) � k,, Saifl t �� '� ....?. . L ., �<}. .w. _�"as Matrix Code i:t d LY,a k r 9-1crZr .pGr�Zx(CHeittD zo s 7-0,2Sr g: 00 sou- n. k 14oL.--1) IP 2 2 vp4m—Z-51, tog F; 03 x II s■ • w 2 3 .-a vrz-o-z—z.,2)N 9.: D 1404 24 s z-t—zo s $: L3 tioca 2-5 --zo s 'Y /G � = e-ki LI) 1-6 vriz.—`l--el , o • IIIP NoL_D 4. 2 7 fez-e-z- ZoN 9; .3d ammo Hou) • 28 . v-z—i—zrs 7 3s Q (4oLp 29 -t-Mgz-o-z-Cog 9.5 ..p 40 • if, 0 t -o-'L- zos .7. g 0 Matrix Codes* �. �" Time S SoiVSolld Sediment SW Surface Water A- none I- Ice GW Ground Water SL Sludge & HNO, 0. Other WW Waste Water 0 Other Spedly) C• M- Me0H �� 3 M, (Please H,SO. DW Drinking Water D- NaOH E- HCI /' Q , I 1 •0. ', 7 QA/QC level with report None 1 23 See price guide fora plicabie fees 0 IR / 1F 7 ` 7^ Pit` T.A.T. Request FDEP _Standard SFWMD_ Rush Date Required Temp Control: / �^ —ter , C e 'C Jupiter Environmental Laboratories, Inc. _ 1Mf1 (IA nt..k. who... _I..wNs. et 97AGO ri 1 A 0 1 r1 r` u re.•.% - ........ •_-,• --- .... . Chain of Custody Record Jupiter Environmental Laboratories J.E.L. Log # f 5 1 L P.O. # Quote# Company Name Al 1 4- .s ae Address 44 Fi - 4 z:,„ % • • Ci xek City lici. P . /J ► State 7-.L. Zip % 3 `t / ( a € ,, � / P. Sampling Site Address >t Attn: 2 A 1/1/P Ag/1%etiZip:rFex/Emeit e4 Protect -.O � Name J�JJI��%l%�Dlect e (�©/% 3 �.� '� Sampler P Name/Signature � ` n t I. �` .tn Comments #". ShPhptl' Ilbat'"� E " N t (C)Ierit,;i�,�,., �z s - �z+� Mntrix Code z idA_ VO �L L1 z-Z-- -zo1ki y-r7-cgs' /o_ lz sn+ i. 1 I/ _� _ Ho c_p 12 AWz Z-'-/os /c: 1s I. v C 3 r z-q-z o5 !o - 30 ( ,. CO 34 sioGzZ-o_z-Zou /o:Ys I <. E4oCB n 15 .>A''60z - Z-qb zN o= /`t(• 1 ✓ -3 0> al.__ 6 s$ z-a-z-low 11: is 1 �. 'ir �) rn (.10 t-r> 17 z-'i—lo tv! / /'- !$ 1 1"' f-lo-:� L. 38 „IFtez-o-Z`1e,S i/-ZS 1 ..... .4 i 9 CZ -0-2-z. //: LFs i , V} ✓ - V ... ----1 (-lbc-• c) ` /j3—, S GW WW DW Matrix Codes* Sediment SW Surface Water lid Water Ground Ground Water SL Sludge Waste Water 0 Other (Please DrinkingWater Specify) ..a. A• nano 1• Ice C• HtSO M• McOr C- 11404 M- Me0H D- NaOH E- HCI �� (� 1 i I r II Date Time � � ,3`/ s Z; IS— ..... r b2, 'DG 0 0None QA/QC level with report _.-_1 __2_,.,3_..., See price guide for applicable fees •^ "b k4 0 ^ f?' 'oj`7 5•1 _A�_ .2, t -L 7 / ? l/ T.A.T. Request FDEP_ _ Standard SFWMD Rush Date Required �,•• Temp Contrro):- ;-ct' .0 Jupiter Environmental Laboratories, Inc. i R'n nbi nivla MI,,kwa , _ r... ... CI r1 1 A Q r) i • Chain of Custody Record BAR t�c3i�ti r:- Juaiter Environmental Laboratories J.E.L. Log # P.O.# Quote# Company Name Alt S ,A • : Address � � /t /y City w P, �o State �6' Zip j/ �/ 0. 10 Ct Sampling Site Address Ale �7�'�+2'` 4� Attn: !% ay/Email P N met o0,6 ! /2,Pr act 0 g©/ 5' 4L 5 r Q3 M1' ? Comments Sampler Name/Signature —/ k la N" Sempl6 abel we a fir. " (Client:to,. .�,. ,....4 . , , _ " ,II . Matrix Code` ..,. 14 1 S4r-aI —Z.—q 3-r. OS—t �. �% Fri = ' u _2 ss z.-a--z-s7 ° r2:Y3 ( vk • • v • j3 5az -o-a ; z:q ( ✓ mink c N _14 sorre,t z-y-574c EZ '• `/, 1 R, ` j "' 7 a5 ssertz z-te-z5 rzss t : v a C) .16 Sa zro-2- t3=0o r L. Z 4.t► .17 6aN o-z- t 3: /o 1 £' 1 -Q • . i 0 . $ SS 'Z-o-2-SN( / 3 :: /S , v Ey .4) - 1 19 5e Z -0 Z->!D l- f 3 =1 e t I m ✓ O ■ ,6o sa z -Z-egos i : L. I t`� Matrix Codes` S SoiVSolid Sediment SW Surface Water GW Ground Water SL Sludge WW wastewater 0 Other (Please DW Drinking Water Specify) °s+=�UL� k none I• Ice B• HNO, 0- Other C- H2SO4 M• McOH -NaOH EHCI • HCI �'' �! tip.. EbyDate Time A ` �,i �/ 3• i7-Q$" Z: ! .S {/ '/--7;? 46 QA/QC level with report None 1 23 See price guide for applicable fees "" �� 14 n sue+ d -0 „..••" �,, �/. , 1. p )i / -7 /y T.A.T. Request FDEP_ _ Standard SFWMD_ Rush Date Required Temp Control: / .0 Jupiter Environmental Laboratories, Inc. 1t:AMel Irthrtek ui..t•....e.. _t....l, . et **ACC t 4 A (1 7 _ /FR11 57R.lr19A • Fw mct% e7,; A440 ,.._,.__._� _ .... .. rorif Chain of Custody Record Jupiter Environmental Laboratories J.E.L. Log # P.O. # Quote# Company Name t4S4 t: ,,... .-- =,„, .... -,,..... -, ,,„-=,,' ••••`.•••" =-• -:- , ,,,,,.,gz,09 ,, „ ••• •-iqr,t ,, -•.,,, ,, . 1. ' Address j griAtr '74 .g tZOW,S Reoff, '•;',..' ... ' City Wf:Sr Pokm6CY-/. State ri. •.zip ..1..g ka% • ii; , t• ,';,..' ' - .. Sampling Site Address lAt14,11( tkei40 . 4 Attn: ;.4„..(b tiiii.lbaecrApr Fax/Email .., Project if Name ICNI‘eriat'or*A. PrOfeef # • -- i Com ments Sampler Name/Signature ',•)40.4.,e,24/,‘ . ','',;;, •x_ i.E.7i Ctr, 0I.,,„,70. # • , #101` ' ' . .7 : Pliiiiiikg ....,,', 7 , •: i i i i .0. • 0 , -,.,,,..,,,%,,:„„ :".,,, ',-Ijk .4 ,"=,`::: , , , ..:::!' matnx Code.* ., 1 4:, 14 .si 3— a - e s 13:2_, so. 1-- . I , ]:r.,,,, fr,...on.041-0-2,-ws- ....m4 . S 2 maNi',-0--z -.we. (3.33 1 1 . „ f - c--- •,4 , -- -,i '.- .4 -7 .,„.; , . % elot.,2) M 4.3 .53r-OC -o—z •-et, S -S- aCt.4 • ,, , ,f 413 r— , . ,.. 1-6 ., ,5.4 sorrez-/e.tc /3:3e f ..' , - i ...-- A e* C, (5 ..2- sio--cf rrez-z-/oW t3 :4z- I , t...-" f=4:1' At *V- X) M M NO L_ 6 im-o-z,e--s , C C) :..3. t3L.1) POecz-z--s I • - 1- =II 18 1 !P...., (..--' :DC. CLI 01 50= Z -0-24-S5 /3 :- -Lg 557:EZZ. -0--Z.--eohf /4:10 .'r• *.;',. Q = PO Lti m S GW WW Matrix Codes* SolVSolid Sediment SW Surface Water Ground Water SL Sludge Waste Water 0 Other Speedy) ' ' • 1 A- none I- Ice B. HNO% 0. Other C• H2SO4 M- Me0H .1":*i" ..-,,j,„ ' '' :I, ;.I = -f ' ''''r'''''' ,1, .1* -''."' •••••.. , - • ' . , , .,„ , 11-4,.2.4r),.:;,,Z,,,..,- ;:;;,-; ,.. ,11 ' ' ,.071P17- ',.'' -; Date Time / (Please DW Drinking Water D- NaOH QA/QC level with report None 1 2 3 See price guide for applicable fees - % /.,? 414 - / 0 17/4/ T.A.T. Fiequest FDEP Standard SFWMD Rush Date Required Temp Control: *C Ar•-•- ,.. , Jupiter Environmental Laboratories, Inc. i CA MIA rthelek 1.11.1swess• 11,...14.2. GI .1 .2 AGO " A A n • Chain of Custody Record Jupiter Environmental Laboratories J.E.L. Log # I f �:21 •P.O.# Quote# Company NameWA ter �. Address 9C-Dia ` ., :..... City /4). gaL. State FL Zip 3371/ it CL .�I, t1 I- Q„ .- .^ ' �.!. -: O �^- w --„ �+ x : Sampling Site Address ral. -r, Attn: n„ �%�iti.�� � tom// Fax/Email ` A Project Name �NlBtirra)04/e Projects XUlS-5r385-63 ' E Z z Sampler `1-��-t.c/ Name/Signature �` 4r/% Lt- Comments # Sample L�b`�I s � •° „ (ClieftpD1... .......... m u,-� � 1... *p'< � "�'!�� & c r�9atrix Code* , x �. t. �qs r _1 m4..ej 3`31/G4 _2 SBMO19— its-c�-z , 1, fz:oo 5 a , J C?z) _3 SBA f4 sS -2-`f • /z sc. S 1-- 1.--' V r KS 1-4-0 La) __4 >GXG�) IY'1- dsE —O—Z it le S 1r; /.....*". LD _5 INg-zea-e-z /f If S L L-- :3-}o M ® 1-4-c->.t � _7 s' J7_S J->7 Z r r r 3:: S 1.. i/`' -I' ' �_ " I4C) Lb = _8 58z f9-st1-z4I rr fy:zp S •t i..-4— �f % , S --Cj —n 0 . Cy --9 $ O � i = ;sat; ,. ;..' ,4 r=: �, __.0 l' '� r� Matrix Codes' ( 'n� � e , ,•.'' . .. , Date Time S SoIVSolid Sediment SW SuAace Water A- none I• Ice GW Ground Water SL Sludge B- HNO, 0- Other WW Waste Water 0 Other Specify) fy) H,SO, M• McOH /4 ',if'tkte /G : it---!� r'�Y �, • !�#6 /� (Please DW Drinking Water • EHC • HCI ....--- QA/QC level with report None 1 _2._3_ See price guide for a plicable fees T.A.T. Request FDEP_ St dab SFWMD Rush Date Required Temp Control: r_ (� ` •C J Jupiter Environmental Laboratories, Inc. 1R11 A,d 111�ds 1.11..4........ i r, .,.wen r) 01 A 0 C Jup /1 ,_ /1 11 Chain of Custody Record Jupiter Environmental Laboratories Company Name N SA EN6INEEQ'S SCIEr•msl-S Address i Li b SK E es TegvaD city\tiEsr 13iLM 13c14. state FL zo 33111 Sampling She Address MI A M I Nel=A LT) AttTERR) gerAN,DAvii V4t Togynall PrV a Name,/`l AN'Nr F IDDER Name Project# 26IS 137S -03 Sampler / Name/Signature .6v�J cat. _3 (C MW— C I 58EEc IF- 2-5/ 58 REe/9 —w--cs Z r_45Brae i 9 sw - z-44 _5 6 _7 _8 9 _-o y-q-d. S Soil/Soid Sediment SW Surface Water GW Ground Water SL Sludge WW Waste Water 0 other (Please Specify) DW Drinidng Water Ig3o to /5 / 23D jb/L A- none 1- Ice B- HNO, 0- Other C- H,SO4 M- McOH D• NaOH E- HCI 4. v cD co 1 rn J.E.L. Log # p0.# Quote# 7zus1I i t�usN Nc)c. D Date 1 ,�.., , Time QA/QC level with report None _12_3_ See price guide for applicable fees T.A.T. Request FDEP_ Standard SFWMD_ Rush Date Required Jupiter Environmental Laboratories, Inc. 150 Old Dixie Hlahwev. Junttc r Ft *adSP 0..AOr! Chain of Custody Record BAR WOE Jupiter Environmental Laboratories Company Name RSA Address LIZ— A Sites r/4p City W 1- f ALM Berl.. State FL zip g371/ Sampling Site Address M 119M1 ALD C\/Pr(reeschff t Attn: v 1D V1l-N0SEGltlgfr Fax/Email it-SA--E . Project Name 1tN IGrPr IZt. poFQ Project # $ O I - ''p3 815-"'Q 3 Sampler Name/Signature _2 _3 4 _7 _8 _9 _0 BIer:Cl9—SE--o-2 s5R.EGQ —St:. -2-1. 4i11. S Soil/Solid Sediment SW Surface Water GW Ground Water SL Sludge WW Waste Water 0 Other (Please Specify) DW Drinking Water ttys I300 SO%L - A- none 1• Ice B- HNO, 0- other v n,av� D- NaOH E- MCI -110 CD � 0 Z -rt!-66 / yam' 11 J.E.L. Log # 1y97H P.O.# Quote# Comments t7 0 T —4 0 Date Time QA/QC level with report None _._1 23See price guide for applicable fees T.A.T. Request FDEP� and SFWMO_ Rush Date Required 1 t Temp Control: ► �G °C Jupiter Environmental Laboratories, Inc.. 150 Oki Dixie Highway, Jupiter, FL 33458 (5611575-0030 • Fax (5611575-411R • irrnitarlbheeholton„+h ne+ C.O.C.# 26160 BAR CODE Chain of Custody Record Jupiter Environmental Laboratories Address I li& A skrotsp.04p City \ r 104, State FL Zip 33411/ MIS ( ALD Sampling Site Address Attn: tp Vats - Project Kf4t6wr Name VAwtF Sampler Name/Signature rij, +PEt6z4f 2 Fax/Email Project # $O /, ii3—0 3 Matrix Codes` S Soll/Solld Sediment SW Surface Water GW Ground Water SL Sludge WW Waste Water 0 Other (Please Specify) DW Drinking Water QA/QC level with report None ,,,_1 _2__3__ See price guide for T.A.T. Request FDEP_ Standard SFWMO_ Date Required /2 : Z8 /:2 2 1=50 A• none I- Ice B• HNO, 0- Other C• H2SO4 M- McOH D• ryaOH E- HCI applicable fees Temp Control: LAB USE ONLY Jr[ /.S�CY[ Jupiter Environmental Laboratories, Inc. 150 Old Dixie Highway, Jupiter, FL 33458 J.E.L. Log # i5 c:jC1 P.O.# Quote# Comments C.o.C.# 2 6 ... 8 /gR11 g7r;_nrY411 • Fov /C011 G7C_A110 BAR CODE tAS USE ONLY Chain of Custody Record Jupiter Environmental Laboratories Company Name tko4 Address 14.157.0-4 .Seloies 18243. City tt&S-1-PAicio Red. Sampling Site Address Attr:1)4't (D VANW6gWir Project I/ _ Name F-NigHr E DpAt Sampler Name/Signature # SainOkt Project 0 _I 4 (5 6 7 8 —9 tv\W-13Z (1PVP) WAC-53 SW -A SW-13 sJ- Matrix Codes" S Soil/Solid Sediment GW Ground Water WW Waste Water DW Drinking Water State FL. Zip 33 4 l4 a Mol.4( AErALD 1:)\1"moraivArre FaxEmail iisfrgtArePis* ko Z. 4.36PS---0-3 SW Surface Water SL Sludge 0 Other (Please Specify) Z)20 3: pc 42:5 4:az A- none 1. Ice B- HNO3 0- Other C- H3S0, M- Me0H D- NaOH E- MCI QA/QC level with report None 1 2 3 See price guide for applicable fees OOP NA; c.•-••••' L!" "1:7 co r 33 rrr o 4; C3 AF27'3M0 t'dVS. 2' • rn C31 —4 rr :Y‹ J.E.L. Log # (A1.51 P.O. # Quote# Comments• Date Time rincs-s" T.A,T. Request FDEP S SFWMD Rush Date Required Temp Control: *c Jupiter Environmental Laboratories, Inc. • 150 Old Dixie Highway, Jupiter, FL 33458 15611 S7S-0030 • Fox Mil 575-41111 • flinitariohg: hgalate,i not c.o.c.# 261J-7 -7 _ Chain of Custody Record BAR CODE Jupiter Environmental Laboratories Company Name AM G1s^1Jew' CefENT! ST5 Address / /86 -A SKEES Eo,4D L43 USE ONLY J.E.L. Log # t I( &5l, P.O. # Quote# CityWESTTh.(vf 13e/4. State FL Zip 33/11 Sampling Site Address MI A MI 14EZACT, Ann: D,t:►,/ ID y4PtDfo? r.4 f 1)i Ntezeg d SA-5/4V4se Fax/Email Project y� pp Name &fM I6F�T etDDEX Project # 861.Y3as- -03 Sampler Name/Signature Sample Label (ClientID) EXA5Wg..c 55 _2 3 _4 _5 6 SAW& 1300 S SoilSolld Sediment SW Surface Water GW Ground Water SL Sludge WW Waste Water 0 Other (Please Specify) DW Drinking Water Solt_ R&f A• none Other t HNC), 0- Other C- C• H,S MO, • McOH D- NaOH E- HCI p 0 IS1, 4 /3/S lifcseWeb by a 0. Comments Date Time 2Ze, QA/QC level with report None 1 2i3See price guide for applicable fees T.A.T. Request FDEP_ -"card SFWMD_ Date Required 1 1 Temp Control: <<G °C Jupiter Environmental Laboratories, Inc. 150 Old Dixie Highway, Jupiter, FL 33458 ir. r� .•tip nnnn r..., ice... .-,. a+ ••• ... ... •• C.O.C.# 26033 ORIGINAL CHAIN OF USTODY RECORD Lo9#- tOVO T#$ Quote: oral. 37' Feic. 6$1 ? 13B Page sax USBD6ta04 Container Type Cod Cr AP ns a:, 1.,1 ��.r..1 Fhsz lar:t! L:s, A aV %At 12)cc *tan1P$: $$aP a 403 PIRA tic, On 410 tm fl $o Qu 1 4•!'1 Ar07% a OE $10101,1 :/r.' 1:reit IV OL V1 SLJ SuitY PC Pr Ira CJT AO .'gyppm VA VV'I3:1.00110. $.'1 if.N11ECl{ MI \i'u.: iilafd A .At OW lira.\] /31er O 01101 Cff fi^:AL:at 1%040 $ NP Ini:tazct A. None E. HCL B. HNO3 F, 1,1oOH C. H2G. 2S2Os p, N>iOHSO4 H.NaNaHSOi Pitreirrs Cr.',v.?.. me? tar C PY.i.. r - , . VR'a 'ncat:E WLr.;A.Y I 1n7? :aa::Ry'a...l: s.r,ul, a1i 'roc•.• ..d TnA e04ur::,1" Zrreo Cnn:avaa 15047 c0 C.a 1. It J. N K. 0,C CHAIN OF CUSTODY RECORD USBIosYsrEMs Log# T#s Quote: 3231NW 7th Ave. Boca Raton. Ft. 33431 Company Nacre: Aderes3: Ciry: eme0: prefect NOfl1a 41 $emper Stratum lAkrg‘ 2 S 5:1; MAN I 90 IND] I 3 4 5 eSAR V -o6 ©fa e206, SUS Biosystems, Inc. Telephone: 80$41624LABS or $61-447-7373 Fax: 66-4848 Page•2.of_2_. Rlwisbrt: U$6091 SO4 Container Type Codes CAL• :IC SYr) at rfl• r.,,•reu,ec •ro PI C 'A.rG u,rpm•v epcc L;A_: »a AG tip.be nerve 'A"Ilr.L 1.t• t<A („hai EIS "stay, 4o► *AP 1L•v S?: m r. 1. U.. nfl r. E2amfile: 1 z lox Pla:t:e, t0.^SJ- 9a2 9Aa Jar tno •.ear.4 Mar AF.Y ari"/if PAR .1lalct a•! IIt l9trt.) :•lairs• al; 'i.u41'a "lair•' A(' Alt.t v:!. CV Wr.te• A. None E. HCl I. Ice a. HNO9 F. MttOH J. MCAA C. Ha804 (3• Na2S203 K. MAO' D. NeOH H. NeH$O4 O. Olher b C7 -.110 T t,ab 1JSb'±;lfliy .' Ara: Wr, K'A tirn:a :r:.A::, arum Acect ve rn tht kr7 no. F'Cecf Picas+ .:. I..I:l:tn I2tt;e10.c1.1lifrr atk1 rtl Pro2a • LC1M61n.R 1. c.0.c.a CHAIN OF CUSTODY RECORD LSBtossiiivis Log# 1(a'!51-7/ (ID T#S, Quote: 3231 N W 7th Ave. Soca Raton, FL 33431 Com;eny NEmc: Address: att<,-> r V tRale: Fe):(4. Projaeci p L� � R;dk ProJ 1 1 Sempler 7 8 9 0 D1k t:punea • Pecs - CO _ ,,204 falai US Biosysterns, Inc. Telephone: 888-862-LABS or 661-447-7373 Fax: 888-456-4846 or 561-447-6136 , L Ioo J. MOM K. tew••se O. Other *fee IUA CJb ucto J J J J r '4 • 'S'5 Rw1610A: USBOSIee4 141 teaeY Santa, Pry Pr•pteeame; C Aids cua rover Pt A Pinar wet el. c*ar ter zr4>c'•o Arbor Pip* "ELL A -ater tag Arrow / , 4l ;. ••t.,ne mai :AU R SO JJo,• . acAra Cow• )1 i}. Sad jYm_ Sot SW be Xtep) for Sea, *MOW *AO s Matrix Cosies'. 40 WO ovals, wn ewe altar ao srrl AA" Aroyac kw war SE Stdi+rnt OR 06rbal Yam Ct. CS AU *Airs Wear rE Pelra turf AO h urwr %A. Nocalunra 11 SNunr. WKM MI. IOC U*Ic A AN OW O, rd WW 0 cow ..eftP i nt Derr itoeeef7 None E. HCL B. HNO3 F. WON C. H2SO4 G. Na2S203 setae NOS i mat trove^ Worms cr 1610.:rrf 7rur 4,;,C Pron roti** it iyAa90% ... Ape Maa. MUsp tine/ CoottCdp ores ea,• meae rtar,=Waane? Cations loge, C.O.C.1